|
<html>
2 l, _6 w2 V& I( y @& ~: C8 \# U+ j5 Y& X" i0 O
5 H! L0 u/ x L [8 j
1 j" d$ T5 x( x: G
<head>
) o4 K' M: }/ Z( }& O* a' @0 v- q6 Q# c
<meta http-equiv="Content-Type" content="text/html; charset=gb2312"># T2 y+ X6 N" b/ N: X' p
0 D. M5 m O' [$ C. D<meta name="GENERATOR" content="Microsoft FrontPage 4.0"># A3 z. C0 T9 x' P7 [0 V/ p
8 }1 W; j( c( L4 \6 }& \6 _<meta name=" rogId" content="FrontPage.Editor.Document">
# I5 o( g- h) B( C1 ?4 ~% s* [# b; W( }8 P5 K7 n/ E
<title>本文介绍了一种用Sol</title>! E! [- c* `9 [& T( H
/ i9 J( S M8 N# [; g9 o1 U; X
</head>
; F7 o) Q0 d* a* j& l* `; j+ }. R% P3 \6 P$ n; t ]
( n0 g7 r" d; I$ u0 m
3 ?3 F' R) x# E# ^( l
<body>; M* I: T/ D4 K% w+ D( y: ]
+ D+ o. A% X- o' J
$ G$ ]5 D- }; ?6 u( T1 X" b" s$ I" v/ O
<table border="0" width="100%">
% \2 M) ^: l; ?, j7 x
9 w1 Y' x$ D. S/ Y S N <tr>) E( l2 d3 D$ T. f. L
& O# z* r7 H. [* u u/ `) L <td width="100%"></td>
& @* f- g' W% R' N( l. S5 w* }, c$ g b3 C7 s6 P4 b
</tr>9 {$ k x9 w# \. D, u
% C; R8 K) I# Y( d, @
<tr>
/ {* d7 R! s1 W5 y! K# o8 l. S8 i9 I( L5 `/ d* y
<td width="100%"><span style="mso-bidi-font-size: 12.0pt; font-family: 宋体; mso-bidi-font-family: Times New Roman; mso-font-kerning: 1.0pt; mso-ansi-language: EN-US; mso-fareast-language: ZH-CN; mso-bidi-language: AR-SA"><font size="2">
# m8 }5 q% [1 S. G5 J5 {1 `" \4 ?
) ]0 G# J2 h* N k 本文介绍了一种用<span lang="EN-US">Sol-Gel方法制备透明纳米TiO<sub>2</sub>薄膜,并在薄膜表面上形成光栅。体现全息图像的光栅条纹是用激光微雕的方法预先制好,并复制到金属镍板上,再在专用的模压机上将光栅条纹复制到TiO<sub>2</sub>薄膜上,利用入射光在表面光栅上的衍射效果可再现激光全息图像。用扫描电镜(SEM)表征了薄膜的表面形貌;用原子力显微镜(AFM)测量了光栅的深度测试了这种结构表面的衍射特性并结合材料的制备对结果进行了分析。</span></font></span></td>' {) Q8 p9 v$ X- T& d5 }
S/ v W" ]9 o/ ]5 n8 H
</tr>
: R! Z4 _: B& q/ }: G5 X/ l7 z* q) o% Y% f+ W4 W
<tr>/ ^6 h# G' C; D2 U
1 q9 w3 ~/ d; Y6 l
<td width="100%">3 [! {1 O5 c1 q& P2 m6 \4 O: s; ~: n
) v+ H- l" Y# V2 t, K R9 z
<p class="MsoBodyText" style="margin-right:1.45pt"><font size="2"><b><span lang="EN-US">Abstract<span style="mso-tab-count:1">
' h5 g% Y/ m5 A$ E* {: A! x$ L8 Y7 g, ?: n" e, [
</span></span></b><span lang="EN-US">The
$ j+ f$ y& C; w8 u2 D( M$ r7 y7 i9 Z7 F1 r! e
surface relief gratings can appear laser hologram pattern on a transparent % d0 b p$ c- `
$ M7 K3 Y5 s: B2 Q; o! N
nano TiO2 coating when changing the angle of view. The coating was made
7 ^) d( i" D+ Q3 m9 ^. K9 a
+ ^4 T, I3 C# a3 n& D1 G+ }6 k Sol-Gel method. The surface relief gratings been coped by a nickel pattern * Z% }; Y/ \) Z7 P
' u: }4 s% }) ]3 A$ ]- e plate which made by electrotype. The micro-structures were investigated - a4 d4 o+ ? M8 U2 E' f
- L7 e1 G% o& {" i
using electron scanning microscopy (SEM). AFM photo gave the depth of the % D W! h) R, x9 c" ~, u
: m6 W( _2 {& h) }: e! [ gratings. The properties of coating and surface relief gratings were + L8 X* t4 a! C0 }# T
/ F' ^* i; g% I2 c- i3 e9 j
researched.</span></font></p>' R; t5 C f+ R/ g5 b
+ [3 g2 Z2 T% j j) u8 x <p class="MsoNormal" align="center" style="text-align:center;text-indent:24.1pt;4 F& h' R! @ {: _4 j
4 D- M1 e9 Q; U9 ? umso-char-indent-count:2.0;mso-char-indent-size:12.05pt"><b><font size="2">引言<span lang="EN-US"><o:p>
( d, A( ^- S% \5 x! I, D
2 W3 }: \! }5 _' b </o:p>
6 |- ~+ w" m4 M1 \# c) ^
; x8 J$ v$ K: U, [9 g" N </span></font></b></p>
8 U7 a0 f& o0 }% R/ p# q# H- H' W# x) \
<p class="MsoNormal" style="text-indent:21.0pt;mso-char-indent-count:2.0;- o( c5 B# x J5 {( f
; j! C$ F2 l+ }1 v% n8 rmso-char-indent-size:10.5pt"><span style="mso-bidi-font-size: 12.0pt"><font size="2">利用薄膜光栅再现激光全息图像的技术早已在防伪制品领域中被广泛应用<sup><span lang="EN-US">[1]</span></sup>。这种薄膜一般是金属或镀有金属具有高达<span lang="EN-US">80%提上的反射率,使光栅的衍射效率很高。但是遇到需要透射的特殊场合这种薄膜就体现出了极大的局限性。非金属介质薄膜具有一定的透射率,lifeng<sup>[2]</sup>和K.Hehl<sup>[3]</sup>等人根据的这一特性研制了具有高衍射效率且透明的全介质多层膜光栅。非金属介质薄膜制备大多采用物理的方法,效率比较低。溶胶-凝胶(Sol-Gel)方法制备非金属介质薄膜具有成分均匀可控、合成温度低、生产效率高等特点受到人们愈来愈多的重视和研究<sup>[4,5]</sup>。<o:p>& M5 l2 H2 i! N" D# J
8 |; P7 |, }, y9 Y, c J1 \2 z </o:p>
+ S9 w& m2 Z: Y: P6 d& B p6 e
" G( t% }; i5 ~9 c8 J) Q! z8 } </span></font></span></p>
3 L- m' a1 s' T7 ]* z
/ D/ e E8 O3 s% H6 N4 i <p class="MsoNormal" style="margin-right:.12gd;text-indent:21.0pt;mso-char-indent-count:4 j+ [& c0 x; Y* X& v
- a# e4 a. c& V: N+ `% S
2.0;mso-char-indent-size:10.5pt"><font size="2"><span style="mso-bidi-font-size: 12.0pt">采用溶胶—凝胶方法制备的<span lang="EN-US">TiO<sub>2</sub>薄膜具有纳米多孔结构<sup>[6,7]</sup>,通过</span></span>专用的模压机上将光栅条纹复制到<span lang="EN-US">TiO<sub>2</sub>薄膜上</span><span style="mso-bidi-font-size: 12.0pt">,能有效地复制出精细的反映激光全息图像的光栅,即能入射光进到在<span lang="EN-US">TiO<sub>2</sub>薄膜上清晰地再现预制的激光全息图像。TiO<sub>2</sub>薄膜是透明的,可见光透过率为90%
( v# ~, a4 ~2 w7 h
0 x( B) [7 e! r- B6 s ,TiO<sub>2</sub>薄膜的折射率n能达到1.8上,因此能够在透明的同时可以在一定的视角范围内清晰地展现激光全息图像,在视角60º时效果最好。<o:p>* R6 S D0 u* b$ |" I# `7 T6 |
) c$ t$ B4 m3 j) H$ n) { </o:p>. v8 r' L- t* y
, I$ v9 c! v2 y' g! q1 p </span></span></font></p>
* J2 J2 z# f8 P9 a: I. _
4 s" R. y5 @. F% y1 X) S <p class="MsoNormal" style="margin-right:.12gd;text-indent:21.0pt;mso-char-indent-count:$ G# h2 G8 E/ r, h/ A, {% y& K
0 l" [# k' m5 E1 y* o1 ?
2.0;mso-char-indent-size:10.5pt"><span style="mso-bidi-font-size: 12.0pt"><font size="2">本文就薄膜及光栅的设计、制备和相关性能进行了探讨。<span lang="EN-US"><o:p>
' R& a; f6 }! j. r
/ ^" M! J! \/ [) [, [5 V2 G- _/ G </o:p>' @6 D% W( w: c: X- U# m7 Z
; m$ \) @8 S- R5 a0 t' _/ T; u% M
</span></font></span></p>3 P+ }2 H: y9 }: W" F
* p% Z. t2 a, I. n+ S0 Q <p class="MsoBodyText" style="margin-right:1.45pt"> </p>
/ G% y7 _" N" [! e1 K. r# Y( V8 L0 X
<p> </td>
% }. [) j8 T# a6 L
; x) [: I, V' B6 O% A0 Z; L K </tr>
+ _7 p5 ^( a* x) ?% @2 ~
* X3 Z- K; r7 G8 W8 y</table>3 n5 n T4 \# Q2 H
1 S! `1 _$ _1 @2 O$ B! T7 `
7 ^! q+ L( A' |- W! z! r3 e T$ f% w8 b3 @8 j/ ]8 T+ ^7 O( V
</body>4 d& h. ` G0 J3 W
0 F+ t- a1 Z: z/ C; W1 V5 a: e) K! f3 i: K- |# I4 P- k0 S
- k& _4 e, M4 r+ c2 K/ i
</html>+ d# D. j* Z/ X+ P5 _
8 j1 M1 M* z3 _
2 i5 Y2 ^" o, r) |% r0 u
0 m x+ ~4 C9 y2 c* k, Q: m" {% n </td>* K4 p% T4 Q8 r
# |9 P+ B$ F9 j" y
</tr>5 V! d4 V) y$ F; ^2 u# A# F; n
y2 I' i& h7 V( x <tr>
: M4 g/ K8 O" M& I: i) B2 |# W/ V2 X/ N# W! _/ N
<td> </td>
u; d5 J& B8 G+ B! q" t! A) x9 p5 |" P0 B. h* o+ H0 R. n
</tr>3 J2 z8 c6 Y5 m
0 E/ N2 F7 y+ `2 A& |) U T3 _
<tr> |
|